Oct 21, 2018 22:49
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Medical: Pharmaceuticals
3.2.S.3.1.2.9. Thermal Behavior
As shown in Figure 13 and Figure 14, no endothermic peak due to the melting of ХХХХ was observed by differential scanning calorimetry (DSC) because it was amorphous. Weight decrease due to the decomposition of isavuconazonium sulfate was observed above 140°C by thermogravimetry (TG).
Figure 13. DSC Curve of Isavuconazonium Sulfate
X-axis: Temperature (°C)
Y-axis: Heat Flow (mW)
[Figure caption:] Exo Down
As shown in Figure 13 and Figure 14, no endothermic peak due to the melting of ХХХХ was observed by differential scanning calorimetry (DSC) because it was amorphous. Weight decrease due to the decomposition of isavuconazonium sulfate was observed above 140°C by thermogravimetry (TG).
Figure 13. DSC Curve of Isavuconazonium Sulfate
X-axis: Temperature (°C)
Y-axis: Heat Flow (mW)
[Figure caption:] Exo Down
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4 | см. | Nina Nikitina |
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Это означает, что на термограмме экзо-эффект пишется вниз, а не вверх.
На всякий случай пояснение: http://www.pinmatlab.com/2014/04/28/directions-of-dsc-heat-f...
На всякий случай пояснение: http://www.pinmatlab.com/2014/04/28/directions-of-dsc-heat-f...
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